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The Influence of Thermal Treatment on the Formation Mechanism of the Cu, Fe-Containing Nanocomposite Material Synthesized by the Sol--Gel Method

Полная версия: 10.1134/S1063783421020207

Ministry of Education, Science and Technological Development of the Republic of Serbia, /, /

Nikolic V.N.¹, Vasic M.M.², Milikic J.², Mariano J.F.M.L.^3,4

¹Department of Theoretical and Condensed Matter Physics, "VINvCA" Institute of Nuclear Sciences --- National Institute of thе Republic of Serbia, University of Belgrade, Belgrade, Serbia

Department of Theoretical and Condensed Matter Physics, "VINČA" Institute of Nuclear Sciences --- National Institute of thе Republic of Serbia, University of Belgrade, Belgrade, Serbia

²Faculty of Physical Chemistry, University of Belgrade, Studentski trg 12-16, Belgrade, Serbia

Faculty of Physical Chemistry, University of Belgrade, Belgrade, Serbia

³Universidade do Algarve, FCT, Campus de Gambelas,-139 Faro, Portugal

Universidade do Algarve, FCT, Campus de Gambelas, Faro, Portugal

⁴Center of Physics and Engineering of Advanced Materials (CeFEMA), IST, Universidade de Lisboa, Av. Rovisco Pais,-001 Lisboa, Portugal

Center of Physics and Engineering of Advanced Materials (CeFEMA), IST, Universidade de Lisboa, Av. Rovisco Pais, Lisboa, Portugal

Email: violeta@vin.bg.ac.rs, mvasic@ffh.bg.ac.rs, jadranka@ffh.bg.ac.rs, jmariano@ualgt.pt

Поступила в редакцию: 22 сентября 2020 г.

Выставление онлайн: 9 ноября 2020 г.

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The nanocomposite samples, containing copper and iron species in the silica matrix, were prepared by annealing at temperatures up to 1100^oC. The samples were investigated by X-ray diffraction analysis, Fourier transform infrared spectroscopy, and cyclic voltammetry. The results of the performed study depict to the presence of a temperature gradient, which acts on the sample during the annealing treatment in the furnace. For the first time, the influence of the temperature gradient on the formation mechanism of the samples was discussed. Keywords: temperature gradient, nanocomposite, sol-gel, XRD, FTIR.

Подсчитывается количество просмотров абстрактов ("html" на диаграммах) и полных версий статей ("pdf"). Просмотры с одинаковых IP-адресов засчитываются, если происходят с интервалом не менее 2-х часов.

Дата начала обработки статистических данных - 27 января 2016 г.

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