Ershov P. A.1, Salnikov V.D.1, Savin V.V.1, Vorontsov P. A.1, Panina L. V.1,2, Rodionova V.V.1
1Immanuel Kant Baltic Federal University, Kaliningrad, Russia
2National University of Science and Technology MISiS, Moscow, Russia
Email: pershov@kantiana.ru
The microphase layering of the composite at the stage of filament yarn formation and its subsequent effect on FDM-printing (fusion deposition modelling) and properties of printed objects were studied. It was found that with the growth of the percentage content of nanoparticles in the filament, the dimensions of pores and ditches in the filament periphery increase. Appearance of defects in the polymer matrix with the increase of CoFe2O4 (CFO) concentration up to 15% is confirmed by differential-scanning calorimetry (DSC) - an additional peak is formed on the enthalpy variation curves. Despite the fact that the highest content of electroactive phase and the magnetization value were found in the film printed from filament thread with 15% content of CFO nanoparticles, the maximum magnetoelectric coefficient α33=3.2 mV/(cm·Oe) was produced on the printed film with 10% content of CFO, which is due to microphase layering. The produced value of magnetoelectric coefficient is lower in the lamellar composites, however, it is sufficient for use of the composites in biomedicine, and use of the FDM-printing technology provides for the possibility of creating complex structures, such as cellular scaffolds. Keywords: 3D-printing, multiferroics, functional composites, magnetic nanoparticles, fluoroplastic.
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