Laser diagnostics of reverse microemulsions in the process of nanoparticle synthesis
Plastinin I. V. , Dolenko T. A.

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In this work, laser spectroscopy was used to study reverse microemulsions, in which the reaction of ZnS nanoparticle synthesis was carried out. The sizes of the synthesized nanoparticles do not exceed 5 nm. As a result of studying the processes in the reaction medium, it was found that the band of stretching vibrations of HS- ions in the region of 2568 cm-1 is an identification sign of the synthesis of nanoparticles: by its intensity it is possible to determine the stage and completion of the ZnS synthesis. Keywords: nanoparticle synthesis, nanoreactors, laser diagnostics, Raman spectroscopy, reverse microemulsions.
  1. L. Dordevic, F. Arcudi, M. Cacioppo, M. Prato. Nat. Nanotechnol., 17, 112 (2022). DOI: 10.1038/s41565-021-01051-7
  2. I.V. Plastinin, S.A. Burikov, T.A. Dolenko. J. Molecular Liquids, 317, 113958 (2020). DOI: 10.1016/j.molliq.2020.113958
  3. I.V. Plastinin, S.A. Burikov, T.A. Dolenko. J. Molecular Liquids, 325, 115153 (2021). DOI: 10.1016/j.molliq.2020.115153
  4. A.M. Smith, S.M. Nie. Acc. Chem. Res., 43, 190 (2010). DOI: 10.1021/ar9001069
  5. J. Bedia, V.M. Ramos, M.P. Garzon, A.G. Aviles, J.J. Rodriguez, C. Belver. Catalysts, 9 (1), 52 (2019). DOI: 10.3390/catal9010052
  6. M.F. Frasco, N. Chaniotakis. Sensors, 9, 7266 (2009). DOI: 10.3390/s90907266
  7. T.F Yia, Y. Lia, Y.M. Lib, S. Luoa, Y.G. Liua. Solid State Ionics, 343, 115074 (2019). DOI: 10.1016/j.ssi.2019.115074
  8. S. Kumar, A. Jain, S. Panwar, I. Sharma, H.C. Jeon, T.W. Kang, R.K. Choubey. J. Appl. Ceramic Technol., 16, 531 (2019). DOI: 10.1111/ijac.13145
  9. B. Meyer, K. Ward, K. Koshlap, L. Peter. Inorg. Chem., 22, 2345 (1983). DOI: 10.1021/ic00158a027

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