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Influence of functionalization with citric acid on the properties of magnetic nanoparticles Zn_xFe_3-xO₄ (0≤ x≤ 1.0)

Russian version

DOI: 10.21883/PSS.2022.10.54249.391

Kamzin A. S.¹, Caliskan G.², Dogan N.², Bingolbali A.³, Semenov V. G⁴, Buryanenko I. V.⁵

¹Ioffe Institute, St. Petersburg, Russia
²Department of Physics, Gebze Technical University, Kocaeli, Turkey
³Department of Bioengineering, Yi ldi z Technical University, Istanbul, Turkey
⁴St. Petersburg State University, St. Petersburg, Russia
⁵Peter the Great Saint-Petersburg Polytechnic University, St. Petersburg, Russia

Email: ASKam@mail.ioffe.ru

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The effect of surface functionalization with citric acid on the properties of magnetic nanoparticles (MNPs) Zn_xFe_3-xO₄ (x=0; 0.25; 0.5; 0.75; 1.0) synthesized by the hydrothermal method was studied. To study the properties of MNPs, X-ray diffractometry (XRD) and energy dispersive X-ray spectroscopy (EDS) were used. The magnetic properties of the samples and the phase state of MNPs were studied using a physical property measurement system (PPMS) and Mossbauer spectroscopy (MS). It has been established that the sizes of crystallites and the crystal lattice parameter of Zn_xFe_3-xO₄ MNPs change with increasing Zn²⁺ concentration. The low values of the coercive force and the presence of a doublet on the MS indicate the presence of both ferrimagnetic and superparamagnetic components. Keywords: Zn_xFe_3-xO₄ ferrite spinel MNPs, hydrothermal synthesis, functionalization of MNPs with citric acid, crystal structure, magnetic properties, magnetic structure.

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