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Modification of the technique and main characteristics of piezoelectric ceramics BiScO3-PbTiO3
Russian version
Guk E.G. 1, Smirnova E.P.1, Klimov V.N.2, Pankratiev P.A. 1, Zaitseva N.V.1, Sotnikov A.V.1, Mukhin E.E. 1
1Ioffe Institute, St. Petersburg, Russia
2Central Research Institute of Structural Materials Prometey, National Research Centre Kurchatov Institute, St. Petersburg, Russia
Email: esmirnoffa@gmail.com, Ais-berg87@mail.ru, pavel-pankratiev@yandex.ru, nvz47@yandex.ru, andrew.sotnikov2014@yandex.ru, e.mukhin@mail.ioffe.ru
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A modified technique for ceramics manufacturing without forced cooling from high-temperature first stage to the low-temperature second stage is proposed. The effect of the cooling regime between two sintering stages on the piezoelectric constants was investigated.This method was used to synthesize high-temperature piezoelectric ceramics 0.36BiScO3-0.64PbTiO3. Structural and piezoelectric parameters of ceramics were studied. It is shown that the obtained ceramics have a tetragonal structure (P4mm) and a composition close to the morphotropic phase boundary, just like the solid solution synthesized by traditional one-step technique. Ceramics synthesized by modified technique are characterized by high density, up to 97% of theoretical value. The average grain sizes of ceramics are in the range of 0.8-1.0 μm. The obtained value of the piezoelectric constant d33 of samples synthesized by the modified technique reaches 525 pC/N. Keywords: piezoelectric ceramics, two step sintering method, optimization.
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