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The sintering temperature effect on the microstructure and dielectric properties of Bi4Ti3O12 doped with neodymium
Russian version
DOI: 10.61011/PSS.2023.08.56568.88
Zubkov S. V.1, Parinov I. A.2, Nazarenko A. V.3, Pavlenko A. V.1,3
1Scientific Research Institute of Physics, Southern Federal University, Rostov-on-Don, Russia
2I.I. Vorovich Institute of Mathematics, Mechanics and Computer Science, Southern Federal University, Rostov-on-Don, Russia
3Federal Research Center Southern Scientific Center of the Russian Academy of Sciences, Rostov-on-Don, Russia
Email: svzubkov61@mail.ru
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A new set of perovskite-like Bi4-xNdxTi3O12 (x=0.1, 0.3, 0.5, 0.7) oxides were synthesized by the method of high-temperature solid-phase reaction at the temperatures of 1000oC and 1050oC. X-ray diffraction study showed that these compounds are single-phase and have the structure of the Aurivillius phases (AP) family with parameters close to the orthorhombic unit cell corresponding to the space group B2cb (41). The microstructure was studied for all obtained Bi4-xNdxTi3O12 (x=0.1, 0.3, 0.5, 0.7) compositions sintered at temperatures of 1000oC and 1050oC. Its analysis also showed that the crystallites are similar one of AP family and characterized with a lamellar-like shape. The relative permittivity ε/ε0 and the dielectric loss tangent tgdelta were measured as a function of temperature at frequencies in the range of 100 kHz to 1 MHz. Keywords: Aurivillius phases, Bi4-xNdxTi3O12, Curie temperature TC, microstructure, permittivity. DOI: 10.61011/PSS.2023.08.56568.88
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