Physics of the Solid State
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- 2022
Microstructure of spherulitic lead zirconate titanate thin films
Staritsyn M. V.
1, Pronin V. P.
2, Khinich I. I.
2, Senkevich S. V.
3, Kaptelov E. Yu.
3, Pronin I. P.
3, Elshin A. S.
4, Mishina E. D.
4
1Central Research Institute of Structural Materials Prometey, National Research Centre Kurchatov Institute, St. Petersburg, Russia
2Herzen State Pedagogical University of Russia, St. Petersburg, Russia
3Ioffe Institute, St. Petersburg, Russia
4MIREA - Russian Technological University, Moscow, Russia
2Herzen State Pedagogical University of Russia, St. Petersburg, Russia
3Ioffe Institute, St. Petersburg, Russia
4MIREA - Russian Technological University, Moscow, Russia
Email: ms_145@mail.ru, pronin.v.p@yandex.ru, khinitch@gmail.com, Senkevichsv@mail.ioffe.ru, Kaptelov@mail.ioffe.ru, Petrovich@mail.ioffe.ru, elshin_andrew@mail.ru, mishina_elena57@mail.ru
The features of the microstructure of radiant spherulites in lead zirconate titanate thin films are studied using scanning electron and nonlinear optical microscopy by varying the blocks size of the perovskite structure. It is shown that as the spherulite radius (or block size) increases, the rotation angle of the growth axis increases, the rotation angle velocity changes, and the magnitude of the second optical harmonic signal changes. Keywords: Lead zirconate titanate thin films, PZT, scanning electron microscopy, nonlinear optical microscopy, pyrochlore-perovskite phase transformation. DOI: 10.61011/PSS.2023.08.56577.140
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