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High-Pressure Si Phases and the Mutual Orientation of Their Structures. HRTEM Studies

Gordeeva T.^1,2, Kulnitskiy B. ^1,2, Popov M.^1,2, Ovsyannikov D.^1,2, Blank V.^1,2

¹Technological Institute for Superhard and Novel Carbon Materials, Centralnaya 7a, Troitsk, Moscow, Russian Federation Technological Institute of Superhard and Novel Carbon Materials, Moscow, Troitsk, Russia

Technological Institute of Superhard and Novel Carbon Materials, Moscow, Troitsk, Russia

²Moscow Institute of Physics and Technology State University, Institutskiy per. 9, Dolgoprudny, Russian Federation Moscow Institute for Physics and Technology, Dolgoprudny, Moscow oblast, Russia

Moscow Institute for Physics and Technology, Dolgoprudny, Moscow oblast, Russia

Email: gordeeva.ta@phystech.edu

Поступила в редакцию: 12 декабря 2020 г.

Выставление онлайн: 14 марта 2021 г.

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As a result of high-resolution transmission electron microscopy (HRTEM) studies of silicon processed in a planetary mill in the presence of diamond powder, high-pressure phases were found: Si-III, Si-IV and Si-IX; moreover, a Si-IX particle with a length of more than 10 nm was detected by TEM methods for the first time. A study of the mutual orientations of the phases obtained allowed us to propose a scheme of transformations in silicon under pressure. We have shown that the Si-IX phase can be formed from Si-IV. The orientation relationship between Si-IV and Si-IX is established. Keywords: silicon, transmission electron microscopy, plastic deformation, planetary mill, phase transformation.

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Дата начала обработки статистических данных - 27 января 2016 г.

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