Technical Physics Letters
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In situ study of the crystallization kinetics of Al2O3 coatings deposited from aluminum isopropoxide during thermal annealing
Mitulinsky A. S.1, Gaydaychuk A. V.1, Zenkin S. P.1, Pirozhkov A. V.1, Linnik S. A.1
1Tomsk Polytechnic University, Tomsk, Russia
Email: mitulinsky@tpu.ru

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Aluminum oxide exists in several polymorphic modifications, each of which determines a specific set of properties important for protective, thermal barrier, and dielectric coatings. The temperature evolution of the phase composition and microstructure of CVD-deposited Al2O3 coatings obtained from aluminum isopropoxide was investigated during annealing up to 1200 oC. X-ray diffraction and electron microscopy data were correlated to reveal the mechanisms of crystallization and the formation of various polymorphic modifications of Al2O3. Keywords: chemical vapor deposition, thin films, aluminum oxide, corundum, thermal stability.
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